Mettler Toledo PR/SR Operations Instructions Page 21

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19
PR/SR balances Startup procedure
09:20:25
–---- REPRO CHECK ---––-
––––––––– END ––––––––––
03.01.96
PR5002
1114051374
Your entry
Good
1.11 g
1.10 g
1.10 g
3
1.103 g
0.006 g
0.52 %
METTLER TOLEDO
Type:
SNR:
Bal:
ReproSet
1
2
3
n
x
s
s rel
Signature:
........................
Test Calibration Repro
Start
If a printer is attached, the result is automatically recorded.
The printout also shows the "ReproSet" setting specified in the "Weighing" menu
(see section 6.3.2).
Determining the minimum sample weight at the location of the balance
If your measured values have to comply with particular tolerance systems (e.g. pharmacopoeia), you can determine the
minimum sample weight which allows you to meet these requirements at the balance location.
For this you consider the relative standard deviation srel, which indicates the percentage error in the measured value. The
standard deviation s is not suitable for this purpose as it shows only the deviation for the particular weight value.
Weight s srel
10.0 g 0.01 g 0.1%
1.0 g 0.01 g 1.0%
Example 1
Same standard deviation s, but different percentage errors srel, depending on the
sample weight.
Weight s srel
10.0 g 0.01 g 0.1%
1.0 g 0.001 g 0.1%
Example 2
Same percentage error srel despite different sample weights and different standard
deviations s of the individual measured values- The absolute standard deviation s is
thus not suitable for the comparison of the quality of measured values.
Procedure
For all sample weights, define a relative standard deviation (for instance, srel
should always be less than 0.1%).
Perform the ReproCheck function several times and systematically lower the
weight of the test specimen to determine the weight at which you are below the
defined relative standard deviation.
If you can not achieve the specified accuracy, you can adapt the repeatability
under "ReproSet" in the "Weighing" menu (see section 6.2.3) to improve the
relative standard deviation.
If the results are still unsatisfactory, change the conditions at the balance
location. For example, use a draft shield or place the balance on a special
weighing table to minimize the influence of external disturbances.
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